Flexural strength properties and fracture site morphology of fine ceramics at room and elevated temperatures
Ochi Yasuo; Haraguchi Kohji; Ishii Akira; Sasaki Shigemi
Abstract:Four point bending tests were conducted on smooth and Vickers indentation notched specimens of Al2O3 and Si3N4 ceramics at room and elevated temperatures. The effects of surface polishing and grinding on the flexural strength of the smooth specimens of Al2O3 ceramics were studied at room temperature at first. And the detailed observation of fracture surface of the smooth specimens by a scanning electron microscope was carried out in order to specify the defect morphology as the fracture site and to study the relation between defect size and flexural strength at room and elevated temperatures. The fracture toughness evaluation by the indentation strength (IS) method was also studied on two kinds of ceramics at room and elevated temperatures for the Vickers indentation notched specimens under different load conditions. Then, by introducing the assumed equivalent crack length, the general evaluation of the relation between strength and crack size (defect size) for the smooth and notched specimens of two kind of ceramics were tried at room and elevated temperatures under the conditions of this study. Key Words:alumina ceramics, silicon nitride ceramics, flexural strength, fracture site morphology, fracture toughness, IS method, room and elevated temperature, equivalent crack length